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Microstructure and Properties of Ni3Al – TiC Surface Composites Formed on Ni3Al Using Low-Energy High-Current Electron Beam

Konstantin V. Ivanov,Kirill O. Akimov, Evgenia K. Ivanova, Marina G. Figurko

Vacuum(2024)

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Abstract
Using scanning and transmission electron microscopy, X-ray diffraction, profilometry, indentation and friction tests we investigated the microstructure and phase composition formation in the near-surface layer, microhardness, surface roughness, resistance to cracking and wear resistance in Ni3Al intermetallic compound and "Ni3Al base – thin powder TiC coating" system processed with low-energy high-current electron beam (LEHCEB). We revealed the crucial role of TiC particles in different behavior of these materials under LEHCEB irradiation with the surface energy density of 8 J/cm2, accelerating voltage of 30 kV and 10 pulses. The mass fraction of TiC in the near-surface was as much as 22 wt. % after three times surfacing. It was found that the presence of TiC thin layer enabled essential microstructure and phase refinement in the near-surface layer of the surface composites and improvement in microhardness and wear resistance. The density of surface cracks in the surface composites is 1.8 lower with respect to TiC-free Ni3Al and the roughness keeps the same. The advantages of LEHCEB processing of intermetallic compounds with thin powder layers are attractive for possible practical application.
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Key words
Ni3Al,Ni3Al-TiC surface composite,surfacing,low-energy high-current pulsed electron beam (LEHCEB) irradiation,microstructure,phase composition
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