Synthesis of Cyclic Sulfamides Via One Pot Alkylation/Aza-Michael Cascade Reaction

Sofia D. Martynova,Anatoly A. Peshkov,Ekaterina Yu. Levashova, Valeria M. Golub, Margarita S. Avakian,Vladimir V. Sharoyko,Stanislav A. Kalinin,Vsevolod A. Peshkov,Dmitry Dar'in

TETRAHEDRON LETTERS（2024）

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摘要

A straightforward and transition metal-free method for the synthesis of cyclic sulfamides via base-promoted bis-alkylation of tert-butyl (N-alkylsulfamoyl)carbamates N-alkylsulfamoyl)carbamates with electron-deficient allyl bromides is described. All obtained cyclic sulfamides underwent successful removal of tert-butoxycarbonyl protecting group.

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