Synthesis of magnesium-based microparticles using oil cake of plukenetia volubilis (Inca fruit) seeds and study of its radical scavenging activity
Materials Today: Proceedings(2022)
摘要
We prepared and characterized Magnesium based particles using remains of Inca fruit seeds after oil press and then checked its antioxidant activity. Seeds were obtained from the company after 2 different processing methods: dried and baked powder of the oil cake (Inca DP) & seed material that was frozen directly after oil pressing process (Inca FC). These two are remaining by product of the oil pressing process and we extracted them separately with 75% ethanol in water (v/v). Then the extracts were used for Mg based particle preparation and characterized using UV–Visible spectrophotometry, FT-IR spectroscopy and SEM. Finally, DPPH antioxidant property of the extracts and the particles was studied. Extraction process yielded approximately 10% of total weight fruit material and almost 10–15% of the particles yielded from 100 mg of the extract. The UV–Visible spectroscopic analyses showed presence of a maximum absorption peak was observed around 200 – 210 nm and FT-IR analyses confirmed the presence of MgO microparticles. Structural analyses with SEM showed a highly aggregated, irregularly shaped particles. Further while studying the antioxidant potential of extract and microparticles, the Inca FC showed appreciable activity than Inca DP. The antioxidant potential of Mg-Inca FC & DP were better than their respective extracts. In conclusion, the Mg-Inca was successfully prepared and it showed significantly better antioxidant activity than the Inca extracts. Further studies on conversion and stabilization of the Mg-Inca particles into nano form with more stability will help us to identify and improve the biological properties of Inca.
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关键词
Sacha inchi,Metal-based particles,Biological synthesis,Magnesium particles,Antioxidant activity
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