Catalytic condensation of phenol with formaldehyde into BPF on recyclable anchoring sulfuric acid
E3S Web of Conferences(2020)
摘要
A novel solid-acid catalyst (PVC-EDA-SO4H) based on polyvinyl chloride (PVC) were prepared after amination of Ethylenediamine (EDA) and anchorage of sulfuric acid. The as-prepared catalyst was characterized by FT-IR, Element analysis, Chemical titration and Thermal analysis, the results indicated that the sulfuric acid was successfully anchored on PVC. The PVC-EDA-SO4 H showed excellent catalytic performance for the synthesis of bisphenol F, and achieved almost high yield and selectivity (94%) of BPF under the mind reaction conditions. Meanwhile, exhibited excellent reusability without the significant loss after six cycles via simple filtration.
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关键词
catalytic condensation,phenol,sulfuric acid,formaldehyde
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