Efficient and reproducible synthesis of an Fmoc-protected Tn antigen
NEW JOURNAL OF CHEMISTRY(2021)
摘要
This concise total synthesis of the Thomsen-Nouveau (Tn) glycoconjugate was accomplished using a palladium-catalyzed coupling between the glycosyl donor and Fmoc-protected serine acceptor. This is, to the best of our knowledge, the shortest synthesis reported from galactose for preparing this essential building block for large-scale solid phase peptide synthesis.
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关键词
antigen,reproducible synthesis,fmoc-protected
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