Solvent-free synthesis of glycosyl chlorides based on the triphenyl phosphine/hexachloroacetone system

Serena Traboni,Federica Liccardo,Emiliano Bedini,Maddalena Giordano,Alfonso Iadonisi

Tetrahedron Letters（2017）

引用 16|浏览9

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摘要

•The hexachloroacetone/PPh3 system allows solvent-free chlorination of hemiacetals.•Glycosyl chlorides can be prepared in high-yields and short times.•Broad compatibility with acid- and base labile protecting groups.

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关键词

Glycosyl chlorides,Solvent-free reactions,Glycosidation,Chlorination,Carbohydrates

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