Cyclic stress response and microcrack initiation mechanism of modified 9Cr‐1Mo steel under low cycle fatigue at room temperature and 350°C

Abstract To investigate the effect of temperature on microcracking mechanisms of modified 9Cr‐1Mo steel, low cycle fatigue tests were performed at 350°C and room temperature (RT). At RT, the cyclic stress response at low strain amplitude (<0.5%) is controlled by friction stress while dominated by back stress at high strain amplitude. By comparison, the disappearance of sub‐grain boundaries induced by dislocation annihilation occurs at 350°C, which contributes to the decrease in back stress, resulting in more significant effects of back stress compared to RT. As a result of the accumulated fatigue damage, the distance between two parallel extrusions at 350°C is larger than that at RT, which is ascribed to the disappearance of low angle sub‐grain boundaries due to dislocation annihilation at 350°C. Due to the disappearance of small‐angle grain boundaries at 350°C, microcracks initiate along high‐angle grain boundaries at 350°C instead of along low‐angle grain boundaries at RT.