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Pd(II)‐catalyzed Carbonylative Cyclization of N‐aryl‐2‐aminopyrimidines with Mo(CO)6 As Carbon Monoxide Source

Ting-Ting Deng,Jie Huang,Guo Lian,Wen-Wu Sun,Bin Wu

Asian Journal of Organic Chemistry（2021）

Cited 3|Views7
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Abstract
A convenient and efficient synthetic protocol for the preparation of pyrimidoquinazolinone through Pd(II)‐catalyzed carbonylative cyclization of N‐aryl‐2‐aminopyrimidines with Mo(CO)6 as carbon monoxide source is established. A series of 6H‐pyrimido[2,1‐b]quinazolin‐6‐one derivatives were obtained in good yields. The scale‐up synthesis was investigated.
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Key words
Pd(II)-catalyzed,carbonylative,cyclization,molybdenum hexacarbonyl,pyrimidoquinazolinone
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