5-甲基-4-(1-氮杂环丙基)吡咯并三嗪-6-甲酸乙酯的合成及表征
Journal of Shaanxi Normal University (Natural Science Edition)(2015)
Abstract
以3-甲基-2-氰基吡咯-4-甲酸乙酯为原料,经3步反应合成了一个含吡咯并三嗪母核结构的新颖化合物5-甲基-4-(1-氮杂环丙基)吡咯并[2,1-f][1,2,4]三嗪-6-甲酸乙酯。通过对其合成过程中的反应条件优化,三步反应以总收率43%制得目标产物。反应所及中间体和最终产物通过1 H NMR、13 C NMR、HRMS、FTIR 进行了结构表征。
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Key words
synthesis,pyrrolotriazin,characterization
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