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新型含吲唑环嘧啶衍生物的合成

ZHANG Xiao-kai,LIU Bing-ni,WANG Ping-bao,LIU Mo,LIU Deng-ke

Chinese Journal of Synthetic Chemistry（2012）

Cited 22|Views8
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Abstract
以6-硝基-1H-吲唑为原料,经氮原子甲基化、催化氢化还原、亲核取代以及烷基化反应制得关键中间体N-(2'-氯嘧啶-4'-基)-N,1-二甲基-1H-吲唑-6-胺(5);5与芳香胺进行亲核取代反应合成了一系列新型取代氨基嘧啶衍生物———N-(2'-取代氨基嘧啶-4'-基)-N,1-二甲基-1H-吲唑-6-胺,其结构经1H NMR和MS表征。
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Key words
1-dimethyl-1H-indazol-6-amine,6-nitro-1H-indazole,synthesis,nuclephilic substitution,N-(2′-chloropyrimidin-4′-yl)-N
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