A new and efficient electrosynthesis of 2-substituted 1,1-cylopropanediylbis(phosphonates)

Sophie Goumain,P Jubault,C Feasson,N Collignon

SYNTHESIS-STUTTGART（1999）

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摘要

Various 2-substituted cyclopropanediylbis(phosphonates) were easily and rapidly prepared under mild conditions in acetonitrile, by electrolysing tetraethyl dichloromethylbis(phosphonate) in the presence of Michael accepters in a two-compartment cell. A particular mechanism was proposed in the case of methyl acrylate.

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关键词

tetraethyl dichloromethylbis(phosphonate),cyclopropanation,Michael acceptors,electrolysis,cyclizations,phosphorus,cyclopropanes

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