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Synthesis of 2'-Deoxy[5'-13C]Ribonucleotides and HMQC-Noesy NMR Study of the Dickerson's Dodecamer with 13C-Labeling at the 5' Positions

Etsuko Kawashima,Takeshi Sekine,Kaoru Umabe,Yuhki Naito,Kazuo Kamaike,Chojiro Kojima,Toshimi Mizukoshi,Ei-Ichiro Suzuki,Yoshiharu Ishido

NUCLEOSIDES & NUCLEOTIDES（1999）

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Abstract
In addition to the synthesis of 2'-deoxy[5'-C-13]ribonucleosides (6) via the D-[5-C-13]ribose derivative (4), the construction of the corresponding dodecanucleotide with the Dickerson's sequence and its HMQC-NOESY NMR analysis are described.
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nmr study,dickerson,synthesis,hmqc-noesy,c-labeling
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