Expeditious and scalable preparation of a Li−Thiele reagent for amine-based bioconjugation

Jiacheng Li,Yuyong Ma,Xiang Zhang,Xin Cao,Hegui Gong,Ang Li

Chinese Chemical Letters（2021）

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摘要

Taking advantage of an arene construction strategy, we developed an expeditious and scalable protocol for preparation of Li − Thiele reagent 1, which may find use in amine-based bioconjugation.

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关键词

Amine-based bioconjugation,Li−Thiele reagent,Arene synthesis,Ortho-phthalaldehyde

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