The Development of a Manufacturing Route to an MCHr1 Antagonist

Michael David Golden,Danny Legg,David Milne, M Arun Bharadwaj, K. Deepthi, Madan Gopal,Nagaraju Dokka,Sudhir Nambiar, Puranik Ramachandra,U. Santhosh,Parhalad Sharma,R. Sridharan,Manjunatha Sulur,Mats Linderberg, Anders Nilsson, Roger Sohlberg, John Kremers, Samuel Oliver, Debasis Patra

ORGANIC PROCESS RESEARCH & DEVELOPMENT（2016）

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摘要

Process development work to provide an efficient manufacturing route to a MCHr1 antagonist is presented herewith. Features of this development work include a scalable manufacturing route to the useful 6-oxa-2-azaspiro[3.3]heptane building block and the use of a (soluble) alternative to sodium triacetoxyborohydride.

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